1,2,3,4,5,6-六氟-双环(2.2.0)己-2,5-二烯合成路线 (共 5 条)
反应条件
chlorine in monofluoro-trichloromethane Irradiation1.) a) ice-bath, b) RT, overnight; Yields of byproduct given;
参考文献
Dailey; Correa; Harrison III; Lemal
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5511 - 5516
反应条件
HOF* CH3CN in acetonitrile T=0°C; 1 h;
参考文献
Wei, Yanjun; Liu, Yufa; Wong, Terrence; Lemal, David M.
Journal of Fluorine Chemistry, 2006 , vol. 127, # 6 p. 688 - 703
反应条件
in gas
P=0.02 Torr; 67 h; Irradiation; Yield given;
参考文献
Dailey; Correa; Harrison III; Lemal
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5511 - 5516
反应条件
oxygen
72 h; Irradiation300 mmHg N2, 200 mmHg O2, vapour phase; Title compound not separated from byproducts;
参考文献
Barlow, Michael G.; Haszeldine, Robert N.; Peck, Colin J.
Journal of the Chemical Society, Chemical Communications, 1980 , # 4 p. 158 - 159
反应条件
oxygen
75 h; Irradiation; Yields of byproduct given;
参考文献
Barlow, Michael G.; Peck, Colin J.
Journal of Fluorine Chemistry, 1993 , vol. 61, # 1.2 p. 179 - 192