N-Boc-DL-苯甘氨醇合成路线 （共 46 条）
反应条件
1: aq. HCl / dioxane; methanol / 1 h / 25 °C 2: Et3N / methanol / 1 h 3: 73 percent / NaOAc; KBr; HOOAc / acetic acid / 3 h / 25 °C View Scheme
参考文献
Synlett, , # 2 art. no. U27404ST, p. 304 - 308
反应条件
1: lithium aluminum hydride / tetrahydrofuran 2: CH2Cl2 View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 19 p. 3069 - 3070
反应条件
1: 1.3 g / SOCl2 / 48 h / Ambient temperature 2: dioxane / 18 h / Ambient temperature 3: DIBAH / CH2Cl2; toluene / 2 h / -78 °C 4: NaBH4 / methanol / 0.5 h / 0 °C View Scheme
参考文献
Synthesis, , # 2 p. 181 - 186
反应条件
1: dioxane / 18 h / Ambient temperature 2: DIBAH / CH2Cl2; toluene / 2 h / -78 °C 3: NaBH4 / methanol / 0.5 h / 0 °C View Scheme
参考文献
Synthesis, , # 2 p. 181 - 186
反应条件
1: DIBAH / CH2Cl2; toluene / 2 h / -78 °C 2: NaBH4 / methanol / 0.5 h / 0 °C View Scheme
参考文献
Synthesis, , # 2 p. 181 - 186
反应条件
1: H2/PdCl2 / methanol / 1 h 2: toluene / 2 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 34 p. 4539 - 4542
反应条件
1: CF3CO2H / CH2Cl2 / 1.5 h / Ambient temperature 2: H2/PdCl2 / methanol / 1 h 3: toluene / 2 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 34 p. 4539 - 4542
反应条件
1: toluene / 2 h / Heating 2: HIO4 / methanol / 1 h / 0 °C 3: NaBH4 / methanol / 1 h / Ambient temperature 4: CF3CO2H / CH2Cl2 / 1.5 h / Ambient temperature 5: H2/PdCl2 / methanol / 1 h 6: toluene / 2 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 34 p. 4539 - 4542
反应条件
1: HIO4 / methanol / 1 h / 0 °C 2: NaBH4 / methanol / 1 h / Ambient temperature 3: CF3CO2H / CH2Cl2 / 1.5 h / Ambient temperature 4: H2/PdCl2 / methanol / 1 h 5: toluene / 2 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 34 p. 4539 - 4542
反应条件
1: concd. HCl / methanol / 1 h / Heating 2: toluene / 2 h / Heating 3: HIO4 / methanol / 1 h / 0 °C 4: NaBH4 / methanol / 1 h / Ambient temperature 5: CF3CO2H / CH2Cl2 / 1.5 h / Ambient temperature 6: H2/PdCl2 / methanol / 1 h 7: toluene / 2 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 34 p. 4539 - 4542
