1.1: triethylamine / diethyl ether / 0 - 20 °C
2.1: osmium(VIII) oxide / tert-butyl alcohol / 0.17 h / 20 °C
2.2: 3 h / 20 °C
View Scheme
参考文献
Harris, Lawrence; Mee, Simon P. H.; Furneaux, Richard H.; Gainsford, Graeme J.; Luxenburger, Andreas
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 358 - 372
1.1: hydroxylamine hydrochloride; sodium carbonate / water / 20 - 45 °C
2.1: triethylamine / diethyl ether / 0 - 20 °C
3.1: osmium(VIII) oxide / tert-butyl alcohol / 0.17 h / 20 °C
3.2: 3 h / 20 °C
View Scheme
参考文献
Harris, Lawrence; Mee, Simon P. H.; Furneaux, Richard H.; Gainsford, Graeme J.; Luxenburger, Andreas
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 358 - 372