1,3-双(二苯基膦)丙烷合成路线 （共 42 条）
参考文献
Yamagishi, Takamichi; Ikeda, Satoru; Yatagai, Masanobu; Yamaguchi, Motowo; Hida, Mitsuhiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1787 - 1790
反应条件
potassium hydroxide; potassium carbonate 1) DMSO, 20 deg C, 2) DMSO, 50 deg C, 1 h; Yield given. Multistep reaction;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 1 p. 11 - 26,8 - 22
参考文献
Journal of Organometallic Chemistry, , vol. 409, # 1-2 p. 163 - 170
反应条件
bis(triphenylphosphine)palladium(II)-chloride in methanol; dimethyl sulfoxide
参考文献
Zeneca Limited
Patent: US5521179 A1, 1996 ;
反应条件
CO; sodium carbonate; palladium diacetate
参考文献
Dow AgroSciences LLC
Patent: US6329528 B1, 2001 ;
反应条件
triethylsilane; caesium carbonate; palladium diacetate in tetrahydrofuran; N,N-dimethyl-formamide
参考文献
GILEAD SCIENCES, INC.
Patent: US2004/121316 A1, 2004 ;
反应条件
carbon monoxide; triethylamine; palladium diacetate in ethanol; ethyl acetate
参考文献
Fujisawa Pharmaceutical Co. Ltd.
Patent: US6573274 B1, 2003 ;
反应条件
palladium monocarbide in water; toluene
参考文献
Nippon Shinyaku Co., Ltd.
Patent: EP1156045 A1, 2001 ;
Title/Abstract Full Text Show Details
Nippon Shinyaku Co., Ltd.
Patent: EP1243268 A1, 2002 ;
反应条件
in tetrahydrofuran reaction in a calorimeter under argon;
参考文献
Inorganic Chemistry, , vol. 27, p. 81 - 85
反应条件
in tetrahydrofuran under N2, react. at room temp.; not isolated, identified by (31)P-NMR;
参考文献
Polyhedron, , vol. 12, p. 721 - 730
