反应条件
1: 4-phenyl-3-butyn-2-one With boron trifluoride diethyl etherate in diethyl ether
T=0°C; 0.05 h; Inert atmosphere;
2: 4-ethylidene-2,2,6,6-tetramethyl-3,5-dioxa-2,6-disilaheptane in diethyl ether
T=0 - 20°C; 4 h; Inert atmosphere; Overall yield = 94 percent;
参考文献
Lopez-Reyes, Morelia E.; Lopez-Cortes, Jose G.; Ortega-Alfaro, M. Carmen; Toscano, R. Alfredo; Alvarez-Toledano, Cecilio
Tetrahedron, 2013 , vol. 69, # 35 p. 7365 - 7372