3-(3-丁烯基)-2,4,4-三甲基环己-2-烯-1-酮合成路线 （共 4 条）
反应条件
pyridinium chlorochromate in dichloromethane
T=20°C; Oxidation; 3 h;
参考文献
Boulin; Arreguy-San Miguel; Delmond
Tetrahedron, 2000 , vol. 56, # 24 p. 3927 - 3932
反应条件
1.1: CuI / diethyl ether / 6 h / 20 °C
1.2: 75 percent / aq. HCl / diethyl ether
2.1: 90 percent / PCC / CH2Cl2 / 3 h / 20 °C
View Scheme
参考文献
Boulin; Arreguy-San Miguel; Delmond
Tetrahedron, 2000 , vol. 56, # 24 p. 3927 - 3932
反应条件
1: 1.) aluminium tri-2-butoxide; 2.) 10percent aq.HCl / 1.) 2-butanol, 2 h, reflux
View Scheme
参考文献
Weerdt, Anton J. A. van der; Apeldoorn, Willem; Boelens, Mans; Koenst, Wil M. B.; Heide, Roel ter
Recueil: Journal of the Royal Netherlands Chemical Society, 1981 , vol. 100, # 12 p. 447 - 449
反应条件
Yield given. Multistep reaction;
参考文献
Weerdt, Anton J. A. van der; Apeldoorn, Willem; Boelens, Mans; Koenst, Wil M. B.; Heide, Roel ter
Recueil: Journal of the Royal Netherlands Chemical Society, 1981 , vol. 100, # 12 p. 447 - 449
