1-氧代-1,2,3,4-四氢萘-2-羧酸乙酯合成路线 （共 33 条）
反应条件
1: 51.4 percent / NaBH4 / ethanol / 6 h 2: 94 percent / toluene-p-sulfonic acid / toluene / Heating 3: 91 percent / diisobutylaluminium hydride / diethyl ether; hexane / 1) -40 deg C to room temperature, 2) room temperature, 12 h 4: 87 percent / N-bromosuccinimide, Me2S / CH2Cl2 / 5 h 5: 92 percent / m-chloroperbenzoic acid / CH2Cl2 / 12 h / 0 °C View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Tetrahedron Letters, 1993 , vol. 34, # 5 p. 867 - 868
反应条件
1.1: NaH / dimethylformamide 2.1: aq. HBr 3.1: NaH / tetrahydrofuran; hexamethylphosphoric acid triamide 3.2: tetrahydrofuran; hexamethylphosphoric acid triamide View Scheme
参考文献
Hasegawa, Eietsu; Yamaguchi, Naoto; Muraoka, Hiroyasu; Tsuchida, Hiroyuki
Organic Letters, 2007 , vol. 9, # 15 p. 2811 - 2814
反应条件
1: 51.4 percent / NaBH4 / ethanol / 6 h 3: NaBH4 / methanol / Ambient temperature 4: toluene-p-sulfonic acid / toluene / 4 h / Heating 5: 96 percent / diisobutylaluminium hydride / diethyl ether; hexane / 1) -78 deg C to room temperature, 2) room temperature, 8 h View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410
参考文献
Hueckel; Goth
Chemische Berichte, 1924 , vol. 57, p. 1290
参考文献
Hueckel; Goth
Chemische Berichte, 1924 , vol. 57, p. 1290
参考文献
Hueckel; Goth
Chemische Berichte, 1924 , vol. 57, p. 1290
参考文献
Hueckel; Goth
Chemische Berichte, 1924 , vol. 57, p. 1290
反应条件
sodium tetrahydroborate in ethanol T=-10°C; 24 h; Heating / reflux;
参考文献
INSTITUT NATIONAL DE LA SANTE ET DE LA RECHERCHE MEDICALE (INSERM)
Patent: EP1683790 A1, 2006 ;
Location in patent: Page/Page column 7; 13 ;
EP 1683790 A1
反应条件
1: 51.4 percent / NaBH4 / ethanol / 6 h 2: 94 percent / toluene-p-sulfonic acid / toluene / Heating 3: 91 percent / diisobutylaluminium hydride / diethyl ether; hexane / 1) -40 deg C to room temperature, 2) room temperature, 12 h 4: 87 percent / N-bromosuccinimide, Me2S / CH2Cl2 / 5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 405 - 410
参考文献
Couture,A. et al.
Journal of the American Chemical Society, 1976 , vol. 98, p. 6218 - 6225
