N-(4-甲氧基苯基)胍合成路线 （共 11 条）
反应条件
scandium tris(trifluoromethanesulfonate) in water
T=20 - 100°C; 48 h;
参考文献
Tsubokura, Kazuki; Iwata, Takayuki; Taichi, Misako; Kurbangalieva, Almira; Fukase, Koichi; Nakao, Yoichi; Tanaka, Katsunori
Synlett, 2014 , vol. 25, # 9 p. 1302 - 1306
反应条件
triethylamine in acetonitrile
T=60°C; 24 h;
参考文献
Draeger, Gerald; Solodenko, Wladimir; Messinger, Josef; Schoen, Uwe; Kirschning, Andreas
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1401 - 1403
Title/Abstract Full Text View citing articles Show Details
Solodenko, Wladimir; Broeker, Patrick; Messinger, Josef; Schoen, Uwe; Kirschning, Andreas
Synthesis, 2006 , # 3 p. 461 - 466
反应条件
triethylamine in tetrahydrofuran
T=60°C; 24 h;
参考文献
Solodenko, Wladimir; Broeker, Patrick; Messinger, Josef; Schoen, Uwe; Kirschning, Andreas
Synthesis, 2006 , # 3 p. 461 - 466
反应条件
trifluoroacetic acid in dichloromethane
T=20°C; 6 h;
参考文献
Guisado, Olga; Martinez, Sonia; Pastor, Joaquin
Tetrahedron Letters, 2002 , vol. 43, # 39 p. 7105 - 7109
反应条件
sodium hydride in 1,4-dioxane; N,N-dimethyl-formamide
T=50 - 60°C; 0.333333 h; Inert atmosphere;
参考文献
Li, Zhenyu; Yu, Fang; Zhan, Peng; Shen, Yuemao; Liu, Xinyong; Cui, Lei; Wang, Shouxun
Medicinal Chemistry, 2012 , vol. 8, # 5 p. 928 - 933,6
反应条件
1.1: polymer-supported carbodiimide / CH2Cl2 / 16 h / 20 °C
1.2: 92 percent / tris(2-aminoethyl)amine, polymer-bound / CH2Cl2 / 16 h / 20 °C
2.1: trifluoroacetic acid / CH2Cl2 / 6 h / 20 °C
View Scheme
参考文献
Guisado, Olga; Martinez, Sonia; Pastor, Joaquin
Tetrahedron Letters, 2002 , vol. 43, # 39 p. 7105 - 7109
反应条件
1: With Rink amide resin; diisopropyl-carbodiimide in dichloromethane
14 h;
2: With piperidine in N,N-dimethyl-formamide
3: With trifluoroacetic acid in dichloromethane
参考文献
Robinson, Dale E.; Seth, Punit P.; Jefferson, Elizabeth A.
Synthetic Communications, 2004 , vol. 34, # 15 p. 2743 - 2749
反应条件
1: iron; acetic acid / methanol / 50 °C / |Inert atmosphere
2: nitric acid / ethanol; water / |Reflux
View Scheme
参考文献
Diab, Sarah; Teo, Theodosia; Kumarasiri, Malika; Li, Peng; Yu, Mingfeng; Lam, Frankie; Basnet, Sunita K. C.; Sykes, Matthew J.; Albrecht, Hugo; Milne, Robert; Wang, Shudong
ChemMedChem, 2014 , vol. 9, # 5 p. 962 - 972
参考文献
Ainley; Curd; Rose
Journal of the Chemical Society, 1949 , p. 101
参考文献
King; Tonkin
Journal of the Chemical Society, 1946 , p. 1063,1069
