2,4,4-三甲基-2-膦酰己二酸合成路线 （共 4 条）
反应条件
nitric acid; NH4VO3 in water
T=55 - 60°C; 5 h;
参考文献
Cook, Barry; Dingwall, John G.
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 22, p. 211 - 216
反应条件
1: 76 percent / H2 / PtO2 / ethanol / 7 h / 100 °C / 76000 Torr
2: 83 percent / NaH / dioxane / 1.) r.t., 4 h, 2.) reflux, 2 h
3: 81 percent / conc. HCl / 24 h / Heating
View Scheme
参考文献
Cook, Barry; Dingwall, John G.
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 22, p. 211 - 216
反应条件
hydrogenchloride
24 h; Heating;
参考文献
Cook, Barry; Dingwall, John G.
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 22, p. 211 - 216
反应条件
1: 83 percent / NaH / dioxane / 1.) r.t., 4 h, 2.) reflux, 2 h
2: 81 percent / conc. HCl / 24 h / Heating
View Scheme
参考文献
Cook, Barry; Dingwall, John G.
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 22, p. 211 - 216
