4-羟基-6-甲基-2-吡喃酮合成路线 (共 149 条)
反应条件
in water
2 h; Heatingproportion equimolar;
参考文献
Castillo, Simone; Ouadahi, Hamid; Herault, Valentin
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 7-8 p. 257 - 261
反应条件
1: H2O / Heating; proportion 1/2
2: Heating
View Scheme
参考文献
Castillo, Simone; Ouadahi, Hamid; Herault, Valentin
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 7-8 p. 257 - 261
反应条件
in water
2 h; Heatingproportion equimolar;
参考文献
Castillo, Simone; Ouadahi, Hamid; Herault, Valentin
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 7-8 p. 257 - 261
反应条件
sodium carbonate in water
1 h; Ambient temperature;
参考文献
Kappe, Thomas; Korbuly, Gertraud; Pongratz, Erik
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 3 p. 398 - 403
反应条件
T=120°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
Tetrahedron, 2011 , vol. 67, # 12 p. 2279 - 2286
反应条件
T=130°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
Tetrahedron, 2011 , vol. 67, # 12 p. 2279 - 2286
反应条件
T=125°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
Tetrahedron, 2011 , vol. 67, # 12 p. 2279 - 2286
反应条件
T=138°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
Tetrahedron, 2011 , vol. 67, # 12 p. 2279 - 2286
反应条件
1: triethylamine / dichloromethane / -20 - 20 °C / |Inert atmosphere
2: iron (III) acetylacetonate / tetrahydrofuran; diethyl ether / -78 °C / |Inert atmosphere
View Scheme
参考文献
Sun, Chang-Liang; Fuerstner, Alois
Angewandte Chemie - International Edition, 2013 , vol. 52, # 49 p. 13071 - 13075
Angew. Chem., 2013 , vol. 125, # 49 p. 13309 - 13313,5
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water
72 h; Ambient temperature;
参考文献
Glombik, Heiner; Tochtermann, Werner
Chemische Berichte, 1983 , vol. 116, # 10 p. 3366 - 3374