(3,3,3-三氟丙基)二氯甲基硅烷合成路线 (共 13 条)
反应条件
RhCl(PPh3)3 T=120°C; 12 h;
参考文献
Ojima, Iwao; Fuchikami, Takamasa; Yatabe, Momoko
Journal of Organometallic Chemistry, 1984 , vol. 260, # 3 p. 335 - 346
反应条件
tri-ruthenium(0)dodecacarbonyl T=120°C; 70 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 260, # 3 p. 335 - 346
反应条件
tetrabutylammomium bromide T=105°C; Disproportionation; 24 h; Equilibrium constant; Further Variations:Temperatures;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 113, # 1-4 p. 79 - 87
反应条件
T=40 - 50°C; Inert atmosphere;
参考文献
Ladilina; Lyubova; Semenov; Kurskii; Kuznetsova
Russian Chemical Bulletin, 2009 , vol. 58, # 5 p. 1015 - 1022
反应条件
diethyl ether; water
参考文献
Tarrant et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 6536,6539
反应条件
magnesium in toluene T=60°C; 1 h; other temperature, reaction time; Product distribution;
参考文献
Klokov
Russian Journal of Applied Chemistry, 1998 , vol. 71, # 3 p. 479 - 482
反应条件
in toluene Heatingeffect of concentration, other reagents; Product distribution;
参考文献
Klokov
Russian Journal of Applied Chemistry, 1998 , vol. 71, # 3 p. 479 - 482
反应条件
diethyl ether; water
参考文献
Tarrant et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 6536,6539
参考文献
Kirichenko, E. A.; Ermakov, A. I.; Pimkin, N. I.; Kopylov, V. M.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 7 p. 1576 - 1580,1280 - 1283
反应条件
in toluene Heatingeffect of concentration, other reagents; Product distribution;
参考文献
Klokov
Russian Journal of Applied Chemistry, 1998 , vol. 71, # 3 p. 479 - 482