(2E,4Z,6E)-5-甲基-7-(2,6,6-三甲基-1-环己烯-1-基)-2,4,6-庚三烯醛合成路线 （共 3 条）
反应条件
1: 55 percent / tetrahydrofuran / 0.5 h / 0 °C 2: 79 percent / MnO2 / CH2Cl2 / Ambient temperature 3: 1.) NaH / 1.) THF, 2.) THF, RT 4: 5N aq. KOH / methanol / 1 h / 60 °C View Scheme
参考文献
Tadikonda, Praveen K.; Lacy, James M.; Rigdon, Michael G.; Deluca, Hector F.
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 1 p. 1 - 10
反应条件
1: 55 percent / tetrahydrofuran / 0.5 h / 0 °C 2: 79 percent / MnO2 / CH2Cl2 / Ambient temperature 3: 1.) NaH / 1.) THF, 2.) THF, RT 4: 5N aq. KOH / methanol / 1 h / 60 °C View Scheme
参考文献
Tadikonda, Praveen K.; Lacy, James M.; Rigdon, Michael G.; Deluca, Hector F.
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 1 p. 1 - 10
反应条件
1: 55 percent / tetrahydrofuran / 0.5 h / 0 °C 2: 79 percent / MnO2 / CH2Cl2 / Ambient temperature 3: 1.) NaH / 1.) THF, 2.) THF, RT 4: 5N aq. KOH / methanol / 1 h / 60 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 39, # 1 p. 1 - 10
