in pyridine-D5
reaction in NMR-tube, under N2 with exclusion of air and water;; complicated product mixture, no single organometallic product isolated; monitored by (1)H-NMR-spectroscopy;;
参考文献
Evans,W.J.; Chamberlain,L.; Ulibarri,T.
Journal of the American Chemical Society, 1988 , vol. 110, p. 6423
water-d2; lithium
1.) 750 deg C, 60 min, 2.) 2 d; Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Landro, Frederick J.; Gurak, John A.; Chinn, John W.; Newman, Robert M.; Lagow, Richard J.
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7345 - 7346
