1: 92 percent / n-butyraldehyde; benzoic acid / toluene / 2 h / Heating 2: HCl / H2O 3: 100 percent / SOCl2 4: Burkholderia cepacia lipase PS; Triton X-100; phosphate buffer / H2O / 3 h / 30 °C / pH 7.0 5: 93 percent / SOCl2 / 3 h / Heating 6: 99 percent / NaHCO3 / toluene / 1 h / 0 - 20 °C View Scheme

sodium hydrogencarbonate in ice-water; nitrogen

phosphate buffer; Burkholderia cepacia lipase PS; Triton X-100 in water T=30°C; pH=7.0; 24 h;

in dichloromethane T=20°C;

暂无反应条件数据

1: 92 percent / n-butyraldehyde; benzoic acid / toluene / 2 h / Heating 2: HCl / H2O View Scheme

butyraldehyde; benzoic acid in toluene 2 h; Heating;