1,1,2,3,3-五氟-3-(三氟甲氧基)-1-丙烯合成路线 (共 2 条)
反应条件
1: carbonic difluoride With potassium fluoride in diethylene glycol dimethyl ether
T=5°C; 2 h; Autoclave;
2: perfluoroallylfluorosulphate in diethylene glycol dimethyl ether
T=5 - 20°C; P=5320.36 Torr; 5 h; Autoclave;
参考文献
Wlassics, Ivan; Tortelli, Vito; Carella, Serena; Monzani, Cristiano; Marchionni, Giuseppe
Molecules, 2011 , vol. 16, # 8 p. 6512 - 6540
参考文献
Berenblit,V.V. et al.
Journal of Organic Chemistry USSR (English Translation), 1979 , vol. 15, p. 1264 - 1271
Zhurnal Organicheskoi Khimii, 1979 , vol. 15, p. 1417 - 1425