2-甲基-2-丙基[3-(乙基氨基)-4-吡啶基]氨基甲酸酯合成路线 （共 6 条）
反应条件
1: in ethanol
T=0 - 20°C;
2: With sodium tetrahydroborate in ethanol
T=0 - 20°C; 10 h;
参考文献
Pfizer Inc
Patent: US2004/63938 A1, 2004 ;
Location in patent: Page 5 ;
US 20040063938 A1
反应条件
1: ethanol / 0 - 20 °C
2: sodium tetrahydroborate; ethanol / 10 h / 0 - 20 °C
View Scheme
参考文献
Caron, Stephane; Do, Nga M.; McDermott, Ruth E.; Bahmanyar
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 257 - 261
反应条件
1: dichloromethane / 20 °C
2: ethanol / 0 - 20 °C
3: sodium tetrahydroborate; ethanol / 10 h / 0 - 20 °C
View Scheme
参考文献
Caron, Stephane; Do, Nga M.; McDermott, Ruth E.; Bahmanyar
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 257 - 261
反应条件
1: dichloromethane / 20 °C
2: ethanol / 0 - 20 °C
3: sodium tetrahydroborate; ethanol / 10 h / 0 - 20 °C
View Scheme
参考文献
Caron, Stephane; Do, Nga M.; McDermott, Ruth E.; Bahmanyar
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 257 - 261
反应条件
trifluoroacetic acid in dichloromethane
T=30°C; 72 h;
参考文献
Pfizer Inc
Patent: US2004/63938 A1, 2004 ;
Location in patent: Page 9 ;
US 20040063938 A1
反应条件
trifluoroacetic acid in dichloromethane
T=30°C; 72 h;
参考文献
Caron, Stephane; Do, Nga M.; McDermott, Ruth E.; Bahmanyar
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 257 - 261
