4-丙基-2,6-二甲氧基苯酚合成路线 （共 16 条）
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Hunter; Hibbert
Journal of the American Chemical Society, 1939 , vol. 61, p. 2190,2193
反应条件
1: 44 percent / tetrahydrofuran / 1) -78 deg C, 10 min, 2) RT, 2 h
2: 1) Me3SiBr, 2) LiAlH4 / 1) THF, 10 min, 2) 0 deg C, 30 min
View Scheme
参考文献
Angle, Steven R.; Arnaiz, Damian O.
Journal of Organic Chemistry, 1992 , vol. 57, # 22 p. 5937 - 5947
反应条件
lithium aluminium tetrahydride; trimethylsilyl bromide
1) THF, 10 min, 2) 0 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Angle, Steven R.; Arnaiz, Damian O.
Journal of Organic Chemistry, 1992 , vol. 57, # 22 p. 5937 - 5947
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1921 , vol. <2> 102, p. 42
反应条件
1: colloid/al palladium; diluted alcohol / Hydrogenation
2: aqueous-alcoholic NaOH-solution
View Scheme
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1921 , vol. <2> 102, p. 42
反应条件
2: glacial acetic acid
3: colloid/al palladium; diluted alcohol / Hydrogenation
4: aqueous-alcoholic NaOH-solution
View Scheme
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1921 , vol. <2> 102, p. 42
