9,9’-螺二[9H-芴]-2,2’-二胺合成路线 （共 5 条）
反应条件
tert.-butylnitrite; copper(ll) bromide in acetonitrile T=60°C; 0.5 h;
参考文献
Wu, Fang-Iy; Dodda, Rajasekhar; Reddy, D. Sahadeva; Shu, Ching-Fong
Journal of Materials Chemistry, 2002 , vol. 12, # 10 p. 2893 - 2897
反应条件
sodium tetrahydroborate; palladium on activated charcoal in methanol
T=20°C; 12 h;
参考文献
Thiemann, Frank; Piehler, Torsten; Haase, Detlev; Saak, Wolfgang; Luetzen, Arne
European Journal of Organic Chemistry, 2005 , # 10 p. 1991 - 2001
反应条件
lithium hexamethyldisilazane; 2-dicyclohexylphosphino-1,1'-biphenyl; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran
T=65°C; 15 h;
参考文献
Thiemann, Frank; Piehler, Torsten; Haase, Detlev; Saak, Wolfgang; Luetzen, Arne
European Journal of Organic Chemistry, 2005 , # 10 p. 1991 - 2001
反应条件
concentrated aqueous HNO3 in ethanol; water; carbon; acetic acid
参考文献
Covion Organic Semiconductors GmbH
Patent: EP1053578 B1, 2002 ;
反应条件
1: With hydrogenchloride; sodium nitrite in water
T=0°C; 0.75 h;
2: With potassium iodide in water
Sandmeyer reaction; 16 h;
参考文献
Thiemann, Frank; Piehler, Torsten; Haase, Detlev; Saak, Wolfgang; Luetzen, Arne
European Journal of Organic Chemistry, 2005 , # 10 p. 1991 - 2001
