N-乙酰基-2-氯-2-脱氧神经氨酸甲酯4,7,8,9-四乙酸酯合成路线 （共 51 条）
反应条件
silver(I) salicylate in benzene 17 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 104, p. 221 - 234
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile 24 h; Title compound not separated from byproducts;
参考文献
Shpirt; Kononov; Torgov; Shibaev
Russian Chemical Bulletin, 2004 , vol. 53, # 3 p. 717 - 719
反应条件
in acetonitrile T=22°C; 12 h; Title compound not separated from byproducts;
参考文献
Shpirt; Kononov; Torgov; Shibaev
Russian Chemical Bulletin, 2004 , vol. 53, # 3 p. 717 - 719
反应条件
in acetonitrile 4 h;
参考文献
Orlova, Anna V.; Shpirt, Anna M.; Kulikova, Nadezhda Y.; Kononov, Leonid O.
Carbohydrate Research, 2010 , vol. 345, # 6 p. 721 - 730
反应条件
in acetone 1.) 0 deg C, 12 h, 2.) room temperature, 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Martichonok, Valeri; Whitesides, George M.
Journal of Organic Chemistry, 1996 , vol. 61, # 5 p. 1702 - 1706
反应条件
in acetonitrile Ambient temperature; Title compound not separated from byproducts;
参考文献
Marra, Alberto; Sinay, Pierre
Carbohydrate Research, 1989 , vol. 190, p. 317 - 322
反应条件
4 A molecular sieve; tetrabutylammomium bromide; di(n-butyl)tin oxide 1.) methanol, 2 h, reflux, 2.) benzene, 4d, 25-30 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Murase, Takatoshi; Kartha, K. P. Ravindranathan; Kiso, Makoto; Hasegawa, Akira
Carbohydrate Research, 1989 , vol. 195, # 1 p. 134 - 137
反应条件
4 A molecular sieve; tetrabutylammomium bromide; di(n-butyl)tin oxide 1.) methanol, 2 h , reflux, 2.) benzene, 4 d, 25 - 30 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Murase, Takatoshi; Kartha, K. P. Ravindranathan; Kiso, Makoto; Hasegawa, Akira
Carbohydrate Research, 1989 , vol. 195, # 1 p. 134 - 137
反应条件
in benzene 17 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 104, p. 221 - 234
反应条件
1: 57 percent / dimethylformamide / 12 h / Ambient temperature 2: 71 percent / M sodium methoxide / methanol / 1 h / Ambient temperature 3: 87 percent / 0.1 M sodium hydroxide / 0.5 h / Ambient temperature View Scheme
参考文献
Eschenfelder; Brossmer
Carbohydrate research, 1987 , vol. 162, # 2 p. 294 - 297
