4-甲氧基亚苄基丙二酸二乙酯合成路线 (共 20 条)
参考文献
Chemische Berichte, , vol. 31, p. 2593
Chem. Zentralbl., , vol. 69, # II p. 695
参考文献
Zuccarello,W.A. et al.
Journal of Medicinal Chemistry, 1969 , vol. 12, # 1 p. 9 - 15
参考文献
Kumar, Satish; Kapoor, Kamal K.
Synlett, 2007 , # 18 p. 2809 - 2814
反应条件
1: 86 percent / propan-2-ol / 2 h 2: 38 percent / triethylamine hydrochloride / 3 h / 180 °C View Scheme
参考文献
Ohno; Izumi; Mizukoshi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 5 p. 1780 - 1783
参考文献
Wayne; Cohen
Journal of the Chemical Society, 1925 , vol. 127, p. 458
参考文献
Kumar, Satish; Kapoor, Kamal K.
Synlett, 2007 , # 18 p. 2809 - 2814
反应条件
1: Raney nickel / 100 °C / Hydrogenation
View Scheme
参考文献
Jacques; Horeau
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 228, p. 1873
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tris(pentafluorophenyl)-borane; hydrogen in toluene
T=80°C; P=45004.5 Torr; 24 h; AutoclaveInert atmosphere;
参考文献
Ines, Blanca; Palomas, David; Holle, Sigrid; Steinberg, Sebastian; Nicasio, Juan A.; Alcarazo, Manuel
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12367 - 12369
Angew. Chem., 2012 , vol. 124, # 49 p. 12533 - 12536,4
参考文献
Kumar, Satish; Kapoor, Kamal K.
Synlett, 2007 , # 18 p. 2809 - 2814
反应条件
1: CuCl / diethyl ether / 3 h / ice-bath
2: aq.KOH / 3 h / Heating
3: 75 percent / aq.H2SO4 / 8 h / Heating
4: 60 percent / polyphosphoric acid (PPA) / 1 h / Heating
View Scheme
参考文献
Selvaraj, S.; Rajendran, A. S.; Arumugam, N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 1047 - 1049