二(2,2,2-三氟乙氧基)三苯基膦烷合成路线 (共 14 条)
反应条件
in ethyl acetate
T=70 - 78°C; Mitsunobu Displacement; 18 h;
参考文献
Tang, Xiaoping; Chapman, Charlotte; Whiting, Matthew; Denton, Ross
Chemical Communications, 2014 , vol. 50, # 55 p. 7340 - 7343
参考文献
Lowther, Nicholas; Crook, Polly; Hall, Dennis
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 30, p. 405 - 408
反应条件
water in toluene; acetonitrile
T=31°C; H2(18)O, hydrolysis of a series of phosphoranes derived from Ar3P and ArP(OCH2CF3)2; Mechanism;
参考文献
Lowther, Nicholas; Hall, C. Dennis
Journal of the Chemical Society, Chemical Communications, 1985 , # 19 p. 1303 - 1305
反应条件
in 1,3,5-trimethyl-benzene
T=114.9°C; var. temp.; Rate constantKinetics;
参考文献
Lowther, Nicholas; Crook, Polly; Hall, C. Dennis
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 102, # 1-4 p. 195 - 204