Bettembourg,M.-C.; Brunesseaux,Y.
Bulletin de la Societe Chimique de France, 1963 , p. 2449 - 2451
→
反应条件
CH3MgI in diethyl ether a soln. of Me(t-Bu)2SnI in ether is added to a soln. of tert-butylchloromagnesium in ether; boiling for 13 h;; removal of solvent; rectification; the fraction obtained at 95-106°C (10 mm) is added to CH3MgI in ether; mixt. is boiled for 3 h; rectification;;
参考文献
Girbasova, N. V.; Bogoradovskii, E. T.; Zavgorodnii, V. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1986 , vol. 56, p. 2439 - 2444
Zhurnal Obshchei Khimii, 1986 , vol. 56, p. 2753 - 2760
in diethyl ether a soln. of Me(t-Bu)2SnBr in ether is added to a soln. of tert-butylchloromagnesium in ether and the reaction mixt. is boiled for 15 h with stirring under Ar;; distn.; elem. anal.;
参考文献
Girbasova, N. V.; Bogoradovskii, E. T.; Zavgorodnii, V. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1986 , vol. 56, p. 2439 - 2444
Zhurnal Obshchei Khimii, 1986 , vol. 56, p. 2753 - 2760
