Hickinbottom; Schluechterer
Nature (London, United Kingdom), 1945 , vol. 155, p. 19
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Tolstopjatow; Woroschilowa
Zhurnal Obshchei Khimii, 1945 , vol. 15, p. 571
Chem.Abstr., 1946 , p. 4662
Brandsma, Lambert; Meijer, Johnny; Verkruijsse, Herman D.; Bokkers, Gysbertus; Duisenberg, Albert J. M.; Kroon, Jan
Journal of the Chemical Society, Chemical Communications, 1980 , # 19 p. 922 - 923
copper dichloride in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Campbell, Matthew J.; Johnson, Jeffrey S.
Organic Letters, 2007 , vol. 9, # 8 p. 1521 - 1524
→
反应条件
CH3MgI in diethyl ether a soln. of Me(t-Bu)2SnI in ether is added to a soln. of tert-butylchloromagnesium in ether; boiling for 13 h;; removal of solvent; rectification; the fraction obtained at 95-106°C (10 mm) is added to CH3MgI in ether; mixt. is boiled for 3 h; rectification;;
参考文献
Girbasova, N. V.; Bogoradovskii, E. T.; Zavgorodnii, V. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1986 , vol. 56, p. 2439 - 2444
Zhurnal Obshchei Khimii, 1986 , vol. 56, p. 2753 - 2760
