反应条件
1: 1-bromo-6-chloro-hexane; n-butyl-magnesium chloride With 1-phenyl-1-propyne; copper dichloride in tetrahydrofuran
T=0°C; 0.25 h;
2: 1,1-dimethylethylmagnesium chloride in tetrahydrofuran
T=68°C; 3 h; Further stages.;
参考文献
Terao, Jun; Todo, Hirohisa; Begum, Shameem Ara; Kuniyasu, Hitoshi; Kambe, Nobuaki
Angewandte Chemie - International Edition, 2007 , vol. 46, # 12 p. 2086 - 2089