2-(氟磺酰基)二氟乙酰基氟化物合成路线 （共 46 条）
反应条件
1: With sulfur trioxide T=40 - 60°C; 48 h; 2: With triethylamine 1 h;
参考文献
Thomas, Brian H.; Shafer, Gregory; Ma, Jing Ji; Tu, Ming-Hu; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 8 p. 1231 - 1240
反应条件
in neat (no solvent) ice cooling;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
反应条件
sulfuric acid T=10 - 15°C; P=2100.17 Torr; 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 121, # 2 p. 147 - 152
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
triethylamine 3 h; Heating;
参考文献
Journal of Fluorine Chemistry, , vol. 121, # 2 p. 147 - 152
反应条件
silver fluoride 1.) diglyme, 3h, 35 deg C, 2.) 35 deg C, 3 d; Yield given. Multistep reaction;
参考文献
Journal of Fluorine Chemistry, , vol. 49, # 3 p. 331 - 347
反应条件
silver fluoride 1.) diglyme, -196 deg C, then 1.5 h at 35 deg C; 2.) -196 deg C, then 3 d at 35 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 46, # 1 p. 39 - 56
反应条件
sulfuric acid; sulfur trioxide; triethylamine 1.) 55 deg C - 65 deg C, 2.) reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 69, # 2 p. 145 - 150
反应条件
silver fluoride 1.) diglyme, -196 deg C, then 2 h at 30-35 deg C; 2.) toluene, -196 deg C, then 2 h at 5-8 deg C and 16 h at 18-20 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 46, # 1 p. 39 - 56
