2-(氟磺酰基)二氟乙酰基氟化物合成路线 (共 46 条)
反应条件
sulfuric acid 5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 121, # 2 p. 147 - 152
反应条件
sulfuric acid 5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 121, # 2 p. 147 - 152
参考文献
Doklady Akademii Nauk SSSR, , vol. 159, p. 135 - 137
C. A., , vol. 62, p. 3927
参考文献
Doklady Akademii Nauk SSSR, , vol. 159, p. 135 - 137
C. A., , vol. 62, p. 3927
反应条件
silver fluoride multistep reaction : new polyfluoroalkoxysulfonyl fluorides; competition reaction with o-(CF3)2C6H3CH2Br, C6F5CH2Br;
参考文献
Journal of Fluorine Chemistry, , vol. 49, # 3 p. 331 - 347
反应条件
T=60°C; 1 h; other temperatures and times (0.5 h at 55-70 deg C, 1 h at 90 deg C); Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 46, # 1 p. 21 - 38
反应条件
fluorine; cesium fluoride in CF2ClCF3 T=-80°C; 3 h;
参考文献
Solvay Solexis S.p.A.
Patent: EP1457484 A1, 2004 ;
Location in patent: Page column 6-7 ;
反应条件
fluorine in 1,1,1,2,2-pentafluoro-2-chlorethyl T=-80°C; 3 h;
参考文献
SOLVAY SOLEXIS S.p.A.
Patent: US2004/199009 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
in carbon disulfide mixing at 0°C for 2 h with AlCl3 , used anhydrous benzene , standing for a night , reflux for 2 h;
参考文献
Journal of the American Chemical Society, , vol. 82, p. 6181 - 6188
F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
(i) AlCl3, CS2, (ii) /BRN= 969212/; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 82, p. 6181 - 6188