2-(氟磺酰基)二氟乙酰基氟化物合成路线 （共 46 条）
反应条件
iodine; silica gel; potassium iodide in acetonitrile T=60 - 65°C; 2 h;
参考文献
Xiao, Ji-Chang; Duan, Jian-Xin; Li, An-Rong; Guo, Yong; Chen, Qing-Yun
Collection of Czechoslovak Chemical Communications, 2002 , vol. 67, # 9 p. 1320 - 1324
反应条件
1: With cesium fluoride in various solvent(s) T=-15°C; P=750 Torr; 8 h; 2: With sodium carbonate T=210 - 225°C; 4 h;
参考文献
Thomas, Brian H.; Shafer, Gregory; Ma, Jing Ji; Tu, Ming-Hu; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 8 p. 1231 - 1240
反应条件
sodium carbonate molar ratio of educts = 2:1, vigorous stirring, 8 h, 160-170°C; by-product is removed by heating to 300°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
sodium hydrogencarbonate; potassium iodide in water; acetonitrile T=30 - 40°C; 0.5 h;
参考文献
Cao, Pin; Duan, Jian-Xing; Chen, Qing-Yun
Journal of the Chemical Society, Chemical Communications, 1994 , # 6 p. 737 - 738
反应条件
chloro-trimethyl-silane T=105°C; P=4200.42 Torr; 6 h;
参考文献
US2007/270602 A1, ;
Page/Page column 4 ;
反应条件
1: T=0 - 100.6°C; P=4350.44 - 5925.59 Torr; 18 h; 2: With chloro-trimethyl-silane T=20 - 107.8°C; Heating / reflux; Product distribution / selectivity;
参考文献
US2007/270602 A1, ;
Page/Page column 3-4 ;
反应条件
1: T=0 - 100.6°C; P=4350.44 - 5925.59 Torr; 18 h; 2: With chloro-trimethyl-silane T=20 - 107.8°C; Heating / reflux; Product distribution / selectivity;
参考文献
Sievert, Allen Capron; Sprague, Lee G.
Patent: US2007/270602 A1, 2007 ;
Location in patent: Page/Page column 3-4 ;
反应条件
water; Petroleum ether
参考文献
Belaventsev, M. A.; Sokol'skii, G. A.; Knunyants, I. L.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1965 , p. 1575 - 1577
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1965 , p. 1613 - 1616
C.A., 1965 , vol. 63, p. 17890
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
in petroleum ether with -10°C of H2O at 30-40°C;
参考文献
England,D.C. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 6181 - 6188
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
pyridine T=-20°C; 0.166667 h;
参考文献
Duan, Jian-Xing; Chen, Quing-Yun
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 6 p. 725 - 730
