tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide Electrolysis; at 25°C, at mercury cathode, at -1.2 V;

tetra-n-butylammonium perchlorate; mercury in N,N-dimethyl-formamide T=-34°C; electrolytic reduction; other reagent, potentials; Product distribution;

tetra-n-butylammonium perchlorate; mercury in N,N-dimethyl-formamide T=25°C; electrolytic reduction; other reagent, potentials; Product distribution;

tetramethylmmonium perchlorate; mercury in N,N-dimethyl-formamide T=-34°C; electrolytic reduction; other reagent, temperature, potentials; Product distribution;

in diethyl ether dropwise addn. of soln. of Li-compd. in diethyl ether to etheric soln. of Hg-compd. with stirring at -30°C, warming to -5°C, further stirring for 1.5 h; addn. of H2O (with ice cooling), sepn. of ether phase, drying over MgSO4, destillation (sepn. of ether and diisobutyl mercury), residue is recrystallized from n-pentane, elem. anal.;