hydrogen fluoride T=5 - 6°C; 7.1 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.7 - 8.1 V; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
hydrogen fluoride T=5 - 6°C; 7.1 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.7 - 8.1 V; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
hydrogen fluoride T=7 - 8°C; 8.55 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.1 V - 6.3 V; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 2 p. 193 - 202