1H,1H,5H-八氟-碘代戊烷合成路线 （共 6 条）
反应条件
potassium iodide in diethylene glycol Heating;
参考文献
Shilin, S. V.; Florensova, O. N.; Chernov, N. F.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 8.2 p. 1838 - 1840,1697 - 1699
反应条件
1: 85 percent / aq. KOH / benzene / 1 h / 80 °C 2: 76 percent / KI / bis-(2-hydroxy-ethyl) ether / Heating View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 8.2 p. 1838 - 1840,1697 - 1699
反应条件
methyl iodide T=230 - 240°C; 5 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 28, p. 152 - 158
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 28, p. 163 - 169
反应条件
zinc in N,N-dimethyl acetamide; water T=26 - 33°C; 3.5 h;
参考文献
Daikin Industries, Ltd.
Patent: EP2078709 A1, 2009 ;
Location in patent: Page/Page column 5 ;
反应条件
1: 1) CF3CO3H, 2) SF4
2: 92 percent / BF3 / CH2Cl2 / 1) -60 deg C, 2) 20 deg C, 3 h
3: 60 percent / CH2Cl2 / 1) 0 deg C, 2 h, 2) 20 deg C, 1 h
View Scheme
参考文献
Mironova, A. A.; Soloshonok, I. V.; Maletina, I. I.; Orda, V. V.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 3 p. 530 - 535
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 3 p. 593 - 598
反应条件
tri-n-butyl-tin hydride
2 h; Heating;
参考文献
Puy, Michael Van Der; Belter, Randolph K.; Borowski, Ralph J.; Ellis, Lois A. S.; Persichini, Phillip J.; et al.
Journal of Fluorine Chemistry, 1995 , vol. 71, # 1 p. 59 - 64
