(2E,4Z)-2,4-庚二烯-1-醇乙酸酯合成路线 （共 7 条）
反应条件
pyridine
3 h; Ambient temperature;
参考文献
Descoins, C.; Lettere, M.; Linsrumelle, G.; Michelot, D.; Ratovelomanana, V.
Synthetic Communications, 1984 , vol. 14, # 8 p. 761 - 774
反应条件
1.1: 75 percent / sodium borohydride / ethanol / 3 h / 20 °C
2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C
2.2: tetrahydrofuran / 24 h / 20 °C
3.1: tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Diego, Dennis G.; Cunha, Rodrigo L.O.R.; Comasseto, Joao V.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7147 - 7148
反应条件
1: 82 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating
2: 83 percent / pyridine / 3 h / Ambient temperature
View Scheme
参考文献
Descoins, C.; Lettere, M.; Linsrumelle, G.; Michelot, D.; Ratovelomanana, V.
Synthetic Communications, 1984 , vol. 14, # 8 p. 761 - 774
反应条件
1: Zn, Cu / propan-2-ol
2: DMAP / diethyl ether
View Scheme
参考文献
Chrelashvili, Z. G.; Mavrov, M. V.; Dolidze, A. V.; Voronkov, A. P.; Serebryakov, E. P.
Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 734 - 736
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 766 - 768
反应条件
1: LiAlH4 / diethyl ether
2: Zn, Cu / propan-2-ol
3: DMAP / diethyl ether
View Scheme
参考文献
Chrelashvili, Z. G.; Mavrov, M. V.; Dolidze, A. V.; Voronkov, A. P.; Serebryakov, E. P.
Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 734 - 736
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 766 - 768
参考文献
Cassani, G.; Massardo, P.; Piccardi, P.
Tetrahedron Letters, 1980 , vol. 21, p. 3497 - 3498
反应条件
1: dilithium tetrachlorocuprate / tetrahydrofuran / 20 °C
2: acetic acid
View Scheme
参考文献
Chrelashvili, Z. G.; Mavrov, M. V.; Dolidze, A. V.; Voronkov, A. P.; Serebryakov, E. P.
Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 734 - 736
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 766 - 768
