2-氯-1,3,5-三甲氧基苯合成路线 （共 8 条）
反应条件
PdCl2(Py)2; potassium acetate in toluene T=100°C; 16 h; Inert atmosphere;
参考文献
Kawamorita, Soichiro; Ohmiya, Hirohisa; Iwai, Tomohiro; Sawamura, Masaya
Angewandte Chemie - International Edition, 2011 , vol. 50, # 36 p. 8363 - 8366
反应条件
dihydrogen peroxide; sodium chloride in water; acetic acid; 1,2-dichloro-ethane
T=60°C; 2 h; stereoselective reaction;
参考文献
Mizuno, Noritaka; Kamata, Keigo; Yamaguchi, Kazuya
Catalysis Today, 2012 , vol. 185, # 1 p. 157 - 161
反应条件
silver carbonate; copper dichloride; palladium dichloride in tetrahydrofuran
T=110°C; 24 h;
参考文献
Peng, Xuefeng; Shao, Xiang-Feng; Liu, Zhong-Quan
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3079 - 3081
反应条件
dihydrogen peroxide; acetic acid; lithium chloride in water; 1,2-dichloro-ethane
T=60°C; 2 h; Inert atmosphere;
参考文献
Yonehara, Kazuhiro; Kamata, Keigo; Yamaguchi, Kazuya; Mizuno, Noritaka
Chemical Communications, 2011 , vol. 47, # 6 p. 1692 - 1694
反应条件
thionyl chloride; diethylamine in chloroform
T=0°C; 1 h;
参考文献
Bell, Kevin H.
Australian Journal of Chemistry, 1985 , vol. 38, # 8 p. 1209 - 1221
反应条件
sulfuric acid in acetic acid
参考文献
Kyburz,E. et al.
Helvetica Chimica Acta, 1962 , vol. 45, p. 813 - 819
反应条件
in diethyl ether
-78 deg C to r.t.;
参考文献
Nagel, Ulrich; Nedden, Hans Guenter
Chemische Berichte, 1997 , vol. 130, # 7 p. 989 - 1006
反应条件
in dichloromethane
T=-90 - 20°C; Kinetics; TemperatureReagent/catalyst;
参考文献
Cong, Zhiqi; Kurahashi, Takuya; Fujii, Hiroshi
Journal of the American Chemical Society, 2012 , vol. 134, # 10 p. 4469 - 4472
