(1S,2S,4R)-2-氯降冰片烷合成路线 （共 9 条）
反应条件
AgNO2; SbF5 1.) Freon-113, -30 deg C, 30 min, 2.) -25 deg C, 2 h then 0 deg C, 3 h;
参考文献
Olah, G. A.; Ramaiah, Pichika
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4639 - 4641
反应条件
water; magnesium oxide T=240°C;
参考文献
Schmerling
Journal of the American Chemical Society, 1946 , vol. 68, p. 195,196
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Universal Oil Prod. Co.
Patent: US2448156 , 1944 ;
参考文献
Schmerling
Journal of the American Chemical Society, 1946 , vol. 68, p. 195,196
反应条件
iron tribromide in dichloromethane T=25°C; 2 h; other alkyl halides; also in presence of Fe(CO)5/I2; other solvents and reaction times; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 54, # 13 p. 3028 - 3036
参考文献
Dneprovskii, A. S.; Pertsikov, B. Z.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 2 p. 222 - 227
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 2 p. 250 - 256
参考文献
Komppa; Beckmann
Justus Liebigs Annalen der Chemie, 1934 , vol. 512, p. 172,182
反应条件
hydrogen iodide T=130°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Namavari, Mohammad; Satyamurthy; Phelps, Michael E.; Barrio, Jorge R.
Tetrahedron Letters, 1990 , vol. 31, # 35 p. 4973 - 4976
反应条件
pentacarbonyliron(0); hydrogen iodide; iodine 1.) dichloromethane, 25 deg C, irradiation, 10 min, 2.) 2 h; Multistep reaction;
参考文献
Yoon, K. B.; Kochi, J. K.
Journal of Organic Chemistry, 1989 , vol. 54, # 13 p. 3028 - 3036
反应条件
LiDBB; ethylene dibromide 1.) THF, 30 s, -78 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Freeman, Peter K.; Hutchinson, Larry L.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4705 - 4713
