2-甲基丙烯酰氧乙基磷酸胆碱合成路线 (共 6 条)
反应条件
in acetonitrile T=50°C; Ring cleavage; Amination; 48 h;
参考文献
Browne, Judith E.; Driver, Michael J.; Russell, Jeremy C.; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 5 p. 653 - 657
反应条件
1: diisopropylammonium tetrazolide / CH2Cl2 / 0.33 h 2: 4,5-dichloroimidazole / acetonitrile / 16 h / 20 °C 3: 62 percent / MCPBA / CH2Cl2 / 0.17 h / 20 °C 4: acetonitrile / 24 h / 75 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 5 p. 653 - 657
反应条件
1: Me3NO / acetonitrile / 0.67 h 2: 37 percent / acetonitrile / 48 h / 50 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 5 p. 653 - 657
反应条件
1: 62 percent / MCPBA / CH2Cl2 / 0.17 h / 20 °C 2: acetonitrile / 24 h / 75 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 5 p. 653 - 657
反应条件
1: 4,5-dichloroimidazole / acetonitrile / 16 h / 20 °C 2: 62 percent / MCPBA / CH2Cl2 / 0.17 h / 20 °C 3: acetonitrile / 24 h / 75 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 5 p. 653 - 657
反应条件
in acetonitrile T=75°C; Amination; 24 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 5 p. 653 - 657