反应条件
1: With (2,2,6,6-tetramethylpiperidinyl)MgCl*LiCl; zinc(II) chloride in tetrahydrofuran T=50°C; 3 h; Inert atmosphere; 2: With bromine in tetrahydrofuran; 1,4-dioxane T=-78 - 25°C; Inert atmosphere; regioselective reaction; Further stages;
参考文献
Klatt, Thomas; Roman, Daniela Sustac; Leon, Thierry; Knochel, Paul
Organic Letters, 2014 , vol. 16, # 4 p. 1232 - 1235