反应条件
1: 86 percent / OsO4, N(CH3)3 / H2O; pyridine; 2-methyl-propan-2-ol / 20 h / Heating 2: CH2Cl2; methanol 3: 90 percent / Pb(OAc)4 / benzene 4: 72 percent / p-TsOH / not given / Ambient temperature 5: 85 percent / Raney Ni (Wl) / ethanol; ethyl acetate 6: CH2Cl2 / -78 °C 7: 49 percent / O3, / ethyl acetate; pyridine / -78 °C 8: 83 percent / LiAlH4 / not given 10: propan-2-ol; xylene / 0 °C / Irradiation 11: 71 percent / OsO4, tert-butyl-hydroperoxide, (Et)4NOH / acetone / 50 °C 13: Li-HMDS / tetrahydrofuran / Ambient temperature 14: 80 percent 16: mesitylenesulfonylchloride / pyridine 18: Li / various solvent(s) View Scheme
参考文献
Tetrahedron Letters, , vol. 28, # 25 p. 2863 - 2866
