反应条件
1: 98 percent / LiAlH4 / diethyl ether / 2 h 2: 75 percent / 1.) sudan red, ozone; 2.) Me2S / CH2Cl2; methanol / 1.) -70 deg C, 5 h; 2.) to rt 3: 90 percent / O3 / CH2Cl2; methanol 4: LiAlH4 / tetrahydrofuran / Ambient temperature 5: 92 percent / ZnCl2 / 1,2-dichloro-ethane / 3 h View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 134, # 10,11 p. 1001 - 1024
