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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5,7-二硝基吲哚啉
合成路线
（共 42 条）
62796-78-5
→
反应条件
67932-53-0
5,7-二硝基吲哚啉
反应条件
potassium carbonate in tetrahydrofuran; methanol T=20°C; 3 h;
参考文献
Helgen, Celine; Bochet, Christian G.
Journal of Organic Chemistry, 2003 , vol. 68, # 6 p. 2483 - 2486
1161880-90-5
→
反应条件
67932-53-0
5,7-二硝基吲哚啉
反应条件
water; potassium carbonate in methanol T=20°C;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
1161880-92-7
→
反应条件
67932-53-0
5,7-二硝基吲哚啉
反应条件
water; potassium carbonate in methanol T=20°C;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
70592-63-1
+
1161880-94-9
→
反应条件
1161881-20-4
+
67932-53-0
5,7-二硝基吲哚啉
反应条件
1: C21H31NO8 With 4-methyl-morpholine; isobutyl chloroformate in dichloromethane T=-20°C; 1 h; Inert atmosphere; 2: 2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride With triethylamine in dichloromethane; N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
115545-84-1
+
1161880-94-9
→
反应条件
1161881-11-3
+
67932-53-0
5,7-二硝基吲哚啉
反应条件
1: Ddz-D-Ala-OH With 4-methyl-morpholine; isobutyl chloroformate in dichloromethane T=-20°C; 1 h; Inert atmosphere; 2: 2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride With triethylamine in dichloromethane; N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
→
反应条件
1161881-14-6
+
67932-53-0
5,7-二硝基吲哚啉
反应条件
1: Ddz-L-Trp-OH With 4-methyl-morpholine; isobutyl chloroformate in dichloromethane T=-20°C; 1 h; Inert atmosphere; 2: 2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride With triethylamine in dichloromethane; N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
1161880-94-9
+
39508-04-8
N-({[2-(3,5-二甲氧基苯基)-2-丙基]氧基}羰基)-L-丙氨酸
→
反应条件
1161881-10-2
+
67932-53-0
5,7-二硝基吲哚啉
反应条件
1: Ddz-L-Ala-OH With 4-methyl-morpholine; isobutyl chloroformate in dichloromethane T=-20°C; 1 h; Inert atmosphere; 2: 2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride With triethylamine in dichloromethane; N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
1161880-94-9
+
39508-07-1
alpha,alpha-二甲基-3,5-二甲氧基苄基-苯丙氨酸
→
反应条件
1161881-13-5
+
67932-53-0
5,7-二硝基吲哚啉
反应条件
1: Ddz-L-Phe-OH With 4-methyl-morpholine; isobutyl chloroformate in dichloromethane T=-20°C; 1 h; Inert atmosphere; 2: 2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride With triethylamine in dichloromethane; N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
1161880-91-6
→
反应条件
67932-53-0
5,7-二硝基吲哚啉
反应条件
water; potassium carbonate in methanol T=20°C;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
1161880-94-9
+
47121-49-3
N-[[1-(3,5-二甲氧基l苯基)-1-甲基乙氧基]羰基]-甘氨酸
→
反应条件
1161881-09-9
+
67932-53-0
5,7-二硝基吲哚啉
反应条件
1: Ddz-L-Gly-OH With 4-methyl-morpholine; isobutyl chloroformate in dichloromethane T=-20°C; 1 h; Inert atmosphere; 2: 2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride With triethylamine in dichloromethane; N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Debieux, Jean-Luc; Bochet, Christian G.
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4519 - 4524
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