Goehring, R. Richard; Sachdeva, Yesh P.; Pisipati, Jyothi S.; Sleevi, Mark C.; Wolfe, James F.
Journal of the American Chemical Society, 1985 , vol. 107, # 2 p. 435 - 443
phosphorous pentoxide in methanesulfonic acid
T=80°C; 1 h;
参考文献
Ulysse, Luckner G.; Yang, Qiang; McLaws, Mark D.; Keefe, Daniel K.; Guzzo, Peter R.; Haney, Brian P.
Organic Process Research and Development, 2010 , vol. 14, # 1 p. 225 - 228
samarium diiodide in tetrahydrofuran
T=20°C; 24 h;
参考文献
McAllister, Laura A.; McCormick, Rosemary A.; James, Karen M.; Brand, Stephen; Willetts, Nigel; Procter, David J.
Chemistry - A European Journal, 2007 , vol. 13, # 4 p. 1032 - 1046
1: 50percent NaH / tetrahydrofuran / 25 h / Ambient temperature
2: 62 percent / KNH2 / liquid ammonia; diethyl ether / 1 h / Irradiation
View Scheme
参考文献
Goehring, R. Richard; Sachdeva, Yesh P.; Pisipati, Jyothi S.; Sleevi, Mark C.; Wolfe, James F.
Journal of the American Chemical Society, 1985 , vol. 107, # 2 p. 435 - 443
1: With tetra-N-butylammonium azide in acetonitrile
Inert atmosphereMicrowave irradiation;
2: With trifluoroacetic acid in acetonitrile
Schmidt reaction; P=2068.65 Torr; Microwave irradiationInert atmosphere;
参考文献
Painter, Thomas O.; Thornton, Paul D.; Orestano, Mario; Santini, Conrad; Organ, Michael G.; Aube, Jeffrey
Chemistry - A European Journal, 2011 , vol. 17, # 35 p. 9595 - 9598
