1,1,2,3,3,4,4-五氟-1-丁烯合成路线 (共 5 条)
反应条件
ethylmagnesium bromide; magnesium in toluene 4 h; Heating / reflux; Product distribution / selectivity;
参考文献
US7504547 B2, ;
Page/Page column 3 ;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 13, p. 2329 - 2331
Zhurnal Organicheskoi Khimii, , vol. 13, # 12 p. 2504 - 2507
反应条件
cesium fluoride in diethylene glycol dimethyl ether
T=20°C; 12 h; Title compound not separated from byproducts;
参考文献
Filyakova, T. I.; Zapevalov, A. Ya.; Kodess, M. I.; Kurykin, M. A.; German, L. S.
Russian Chemical Bulletin, 1994 , vol. 43, # 9 p. 1526 - 1531
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 9 p. 1614 - 1619
反应条件
SbF5
T=20°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Filyakova, T. I.; Zapevalov, A. Ya.; Kodess, M. I.; Kurykin, M. A.; German, L. S.
Russian Chemical Bulletin, 1994 , vol. 43, # 9 p. 1526 - 1531
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 9 p. 1614 - 1619
参考文献
Filyakova,T.I. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, p. 635 - 637
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, # 3 p. 681 - 683