3-(2-甲氧基苯氧基)丙醛合成路线 （共 2 条）
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
T=20°C; 2 h;
参考文献
Panchgalle, Sharad P.; Kunte, Sunita S.; Chavan, Subhash P.; Kalkote, Uttam R.
Synthetic Communications, 2011 , vol. 41, # 13 p. 1938 - 1946
反应条件
1.1: p-nitrosobenzene; L-proline / acetonitrile / 24 h / -20 °C
1.2: 0.17 h / -20 °C
1.3: 6 h / 20 °C / 760.05 Torr
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / 1,4-dioxane / 0.83 h / 70 °C
3.1: dichloromethane / 30 h / 20 °C
View Scheme
参考文献
Panchgalle, Sharad P.; Kunte, Sunita S.; Chavan, Subhash P.; Kalkote, Uttam R.
Synthetic Communications, 2011 , vol. 41, # 13 p. 1938 - 1946
