6-乙烯基-1,3,5-环庚三烯-1-甲醛合成路线 (共 1 条)
反应条件
1: 1.) triphenylphosphine / 1) CH2Cl2, 0 deg C, 15 min; 2) CH2Cl2, 30 min, room temperature
2: 86 percent / dimethylformamide / 0.5 h / Heating
3: 84 percent / dimethylformamide / 2 h / Heating
4: 60 percent / DIBAH / toluene / 0.5 h / Ambient temperature
View Scheme
参考文献
Klingensmith, Kenneth A.; Puettmann, Wilhelm; Vogel, Emanuel; Michi, Josef
Journal of the American Chemical Society, 1983 , vol. 105, # 11 p. 3375 - 3380