1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
参考文献
Wang, Changning; Moseley, Christian K.; Carlin, Stephen M.; Wilson, Colin M.; Neelamegam, Ramesh; Hooker, Jacob M.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 11 p. 3389 - 3392
silver carbonate in dimethyl sulfoxide
T=50°C; SolventReagent/catalyst;
参考文献
Wang, Changning; Moseley, Christian K.; Carlin, Stephen M.; Wilson, Colin M.; Neelamegam, Ramesh; Hooker, Jacob M.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 11 p. 3389 - 3392
1.1: pyridine / 1 h / 0 - 20 °C
2.1: potassium tert-butylate / dimethyl sulfoxide / 60 °C
2.2: 1 h / 80 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
View Scheme
参考文献
Wang, Changning; Moseley, Christian K.; Carlin, Stephen M.; Wilson, Colin M.; Neelamegam, Ramesh; Hooker, Jacob M.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 11 p. 3389 - 3392
1.1: pyridine / 1 h / 0 - 20 °C
2.1: potassium tert-butylate / dimethyl sulfoxide / 60 °C
2.2: 1 h / 80 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
View Scheme
参考文献
Wang, Changning; Moseley, Christian K.; Carlin, Stephen M.; Wilson, Colin M.; Neelamegam, Ramesh; Hooker, Jacob M.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 11 p. 3389 - 3392
1.1: potassium tert-butylate / dimethyl sulfoxide / 60 °C
1.2: 1 h / 80 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
View Scheme
参考文献
Wang, Changning; Moseley, Christian K.; Carlin, Stephen M.; Wilson, Colin M.; Neelamegam, Ramesh; Hooker, Jacob M.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 11 p. 3389 - 3392
