N-叔丁氧羰基-1,4-丁二胺合成路线 （共 29 条）
反应条件
in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
McWatt, Martin; Boons, Geert-Jan
European Journal of Organic Chemistry, 2001 , # 13 p. 2535 - 2545
反应条件
1: 100 percent / NaHCO3, NaCl / CHCl3; H2O / 1.5 h / Heating 2: 74 percent / 18-crown-6 / acetonitrile / 14 h / Heating 3: 74 percent / NaBH4, cobaltous chloride hexahydrate / methanol / 1 h / 0 °C View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 28, # 1 p. 65 - 76
反应条件
1: 74 percent / 18-crown-6 / acetonitrile / 14 h / Heating 2: 74 percent / NaBH4, cobaltous chloride hexahydrate / methanol / 1 h / 0 °C View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 28, # 1 p. 65 - 76
反应条件
in dichloromethane T=20°C;
参考文献
Ghanem, Mohamed A.; Chretien, Jean-Mathieu; Pinczewska, Aleksandra; Kilburn, Jeremy D.; Bartlett, Philip N.
Journal of Materials Chemistry, 2008 , vol. 18, # 41 p. 4917 - 4927
反应条件
1: 77 percent / Ph3P, DEAD / tetrahydrofuran / Ambient temperature 2: 83 percent / Zn, 1.) M aq. KH2PO4 / tetrahydrofuran / 4 h / Ambient temperature 3: 95 percent / H2 / 10percent Pd/C / methanol / 1 h / Ambient temperature View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 8 p. 2143 - 2161
反应条件
1: 83 percent / Zn, 1.) M aq. KH2PO4 / tetrahydrofuran / 4 h / Ambient temperature 2: 95 percent / H2 / 10percent Pd/C / methanol / 1 h / Ambient temperature View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 8 p. 2143 - 2161
反应条件
potassium hydrogencarbonate in 1,4-dioxane; water
参考文献
Polish Journal of Chemistry, , vol. 52, p. 1167 - 1172
反应条件
in diethyl ether; dimethyl sulfoxide 1 h; Ambient temperature;
参考文献
Hansen, J. B.; Nielsen, M. C.; Ehrbar, U.; Buchardt, O.
Synthesis, 1982 , # 5 p. 404 - 405
反应条件
in chloroform T=20°C;
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 9 p. 4457 - 4478
反应条件
hydrogenchloride in diethyl ether Yield given;
参考文献
Hansen, J. B.; Nielsen, M. C.; Ehrbar, U.; Buchardt, O.
Synthesis, 1982 , # 5 p. 404 - 405
