methanol in methanol fast addn. of SiCl4 to a small excess of CH3OH (ice bath);; fractional distn.;;
参考文献
Peppard, D. F.; Brown, W. G.; Johnson, W. C.
Journal of the American Chemical Society, 1946 , vol. 68, p. 73 - 75
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Gmelin Handbook: Si: MVol.C, 117, page 329 - 330
methanol in neat (no solvent) heating of Si at 1050°C in H2-atm. for 2 h in presence of Cu-oxide, Cu-halide or Cu-nitrate; dropwise addn. of CH3OH at 300°C;;
