1: methanol; bis-trimethylsilyl ether T=0 - 10°C; 2: With sulfuric acid T=10°C; 0.5 h; 3: orthosilicic acid tetramethyl ester With water more than 3 stages;
参考文献
Kanebo Cosmetics, Inc.; Shin-Etsu Chemical Co., Ltd.
Patent: EP1607081 A1, 2005 ;
Location in patent: Page/Page column 14-17 ;
Amberlyst 15 cation-exchange resin T=40°C; 85 h; further times; variation of the ratios of the educts; further tetralkoxysilanes; Product distribution;
参考文献
Hasegawa, Isao; Sakka, Sumio
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 12 p. 4313 - 4316
