1: With lithium diisopropyl amide in tetrahydrofuran; hexane
0.25 h; Inert atmosphereCooling with acetone-dry ice;
2: With copper dichloride in tetrahydrofuran; hexane
2 h;
参考文献
GEORGIA TECH RESEARCH CORPORATION; GETMANENKO, Yulia A.; MARDER, Seth; HWANG, Do Kyung; KIPPELEN, Bernard
Patent: WO2013/23109 A1, 2013 ;
Location in patent: Page/Page column 41; 42 ;