(2-甲基-6-(三氟甲基)吡啶-3-基)甲醇合成路线 （共 4 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; 3 h;
2: With sodium hydroxide; water in tetrahydrofuran
参考文献
SYNGENTA LIMITED
Patent: WO2007/71900 A1, 2007 ;
Location in patent: Page/Page column 93 ;
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C; 1.25 h;
2: With water; Sodium potassium tartrate in tetrahydrofuran
1.16 h;
参考文献
Wu, Gang; Mikkilineni, Amarendra B.; Sher, Philip M.; Murugesan, Natesan; Gu, Zhengxiang
Patent: US2006/287341 A1, 2006 ;
Location in patent: Page/Page column 42-43 ;
US 20060287341 A1
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C; 1.25 h;
2: With water; Potassium sodium tartrate
0.166667 h;
参考文献
Sun, Chongqing; Sher, Philip M.; Wu, Gang; Ewing, William R.; Huang, Yanting; Lee, Taekyu; Murugesan, Natesan; Sulsky, Richard B.
Patent: US2007/4772 A1, 2007 ;
Location in patent: Page/Page column 78 ;
反应条件
thionyl chloride in dichloromethane
T=20°C; 16 h;
参考文献
SYNGENTA LIMITED
Patent: WO2007/71900 A1, 2007 ;
Location in patent: Page/Page column 93-94 ;
