6-(2-苯并噻唑基)-1-乙基-2-[2-(甲基苯基氨基)乙烯基]-3-苯基-1H-苯并咪唑鎓碘化物合成路线 (共 7 条)
反应条件
T=75°C; 24 h; Inert atmosphere;
参考文献
Sun, Qi; Wu, Runzhi; Cai, Sutang; Lin, Yuan; Sellers, Llewlyn; Sakamoto, Kaori; He, Biao; Peterson, Blake R.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 5 p. 1126 - 1139
反应条件
1: palladium 10 on activated carbon; hydrazine / ethanol / 0.5 h / 80 °C / Inert atmosphere 2: zirconium tetrachloride / ethanol / 0.5 h / 80 °C / Inert atmosphere 3: manganese(IV) oxide / 0.08 h / 22 °C / Inert atmosphere 4: 24 h / 75 °C / Inert atmosphere View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 5 p. 1126 - 1139
反应条件
1: zirconium tetrachloride / ethanol / 0.5 h / 80 °C / Inert atmosphere 2: manganese(IV) oxide / 0.08 h / 22 °C / Inert atmosphere 3: 24 h / 75 °C / Inert atmosphere View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 5 p. 1126 - 1139
反应条件
1: zirconium tetrachloride / ethanol / 0.5 h / 80 °C / Inert atmosphere 2: manganese(IV) oxide / 0.08 h / 22 °C / Inert atmosphere 3: 24 h / 75 °C / Inert atmosphere View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 5 p. 1126 - 1139
反应条件
1: ethanol / 16 h / Reflux; Inert atmosphere 2: potassium carbonate / dimethyl sulfoxide / 8 h / Inert atmosphere; Heating 3: palladium 10 on activated carbon; hydrazine / ethanol / 0.5 h / 80 °C / Inert atmosphere 4: zirconium tetrachloride / ethanol / 0.5 h / 80 °C / Inert atmosphere 5: manganese(IV) oxide / 0.08 h / 22 °C / Inert atmosphere 6: 24 h / 75 °C / Inert atmosphere View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 5 p. 1126 - 1139
反应条件
1: manganese(IV) oxide / toluene / Inert atmosphere 2: zirconium tetrachloride / ethanol / 0.5 h / 80 °C / Inert atmosphere 3: manganese(IV) oxide / 0.08 h / 22 °C / Inert atmosphere 4: 24 h / 75 °C / Inert atmosphere View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 5 p. 1126 - 1139
反应条件
1: ethanol / 16 h / Reflux; Inert atmosphere 2: potassium carbonate / dimethyl sulfoxide / 8 h / Inert atmosphere; Heating 3: palladium 10 on activated carbon; hydrazine / ethanol / 0.5 h / 80 °C / Inert atmosphere 4: zirconium tetrachloride / ethanol / 0.5 h / 80 °C / Inert atmosphere 5: manganese(IV) oxide / 0.08 h / 22 °C / Inert atmosphere 6: 24 h / 75 °C / Inert atmosphere View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 5 p. 1126 - 1139