1,2,3,6,7,8,11,12-八氢苯并[E]芘-9(10H)-酮合成路线 （共 7 条）
反应条件
ethanol; sodium Erhitzen des Reaktionsprodukts mit Selen auf 320-340grad;
参考文献
Cook; Hewett
Journal of the Chemical Society, 1933 , p. 398,401
Chemistry and Industry (London, United Kingdom), 1936 , p. 843
反应条件
Erhitzen des Reaktionsprodukts mit Selen auf 320-340grad;
参考文献
Cook; Hewett
Journal of the Chemical Society, 1933 , p. 398,401
Chemistry and Industry (London, United Kingdom), 1936 , p. 843
反应条件
1: 81 percent / diethylene glycol, hydrazine monohydrate, KOH / 6 h / Heating 2: 85 percent / AlCl3 / benzene / 4 h / Ambient temperature View Scheme
参考文献
Sangaiah, R.; Gold, A.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2620 - 2622
反应条件
1: N2H4, KOH / bis-(2-hydroxy-ethyl) ether / Heating
2: liq. HF
View Scheme
参考文献
Harvey,R.G. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 1 p. 78 - 83
参考文献
Harvey,R.G. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 1 p. 78 - 83
反应条件
1: 88 percent / p-Tosic acid / acetic anhydride / 14 h / Heating
2: 80 percent / DDQ / 4 h / Heating
3: 84 percent / p-Tosic Acid / methanol / 4 h
View Scheme
参考文献
Lee; Shyamasundar; Harvey
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2889 - 2895
反应条件
potassium hydroxide; hydrazine hydrate; diethylene glycol
6 h; Heating;
参考文献
Sangaiah, R.; Gold, A.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2620 - 2622
